6B0E
Crystal structure of Pfs25 in complex with the transmission blocking antibody 1260
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-13 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.223, 79.635, 78.065 |
Unit cell angles | 90.00, 90.91, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.400 |
High resolution limit [Å] | 3.300 | 3.300 |
Rpim | 0.044 | 0.362 |
Number of reflections | 9915 | 835 |
<I/σ(I)> | 14.6 | 1.5 |
Completeness [%] | 99.8 | 100 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 294 | 2.0 M ammonium sulfate, 0.1 M Tris pH 8.5 |