6AUB

CRYSTAL STRUCTURE OF BRUTON'S TYROSINE KINASE IN COMPLEX WITH INHIBITOR CGI2815

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (1.65 Å)

Cell axes108.489108.48942.078
Cell angles90.0090.00120.00
SpacegroupP 61
Resolution limits27.14 - 1.65
the highest resolution shell value1.700 - 1.650
R-work0.16600
the highest resolution shell value0.222
R-free0.19900
the highest resolution shell value0.269

Data Collection Statistics

Resolution limits50.00 - 1.65
the highest resolution shell value -
Number of reflections34147
Completeness99.8
Redundancy5
the highest resolution shell value4.9

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, SITTING DROP7289

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*