6YIO
CRYSTAL STRUCTURE OF FAB RG6292 IN COMPLEX WITH CD25 ECD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.99982 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.381, 44.321, 140.085 |
Unit cell angles | 90.00, 92.41, 90.00 |
Refinement procedure
Resolution | 69.980 - 1.830 |
R-factor | 0.2039 |
Rwork | 0.203 |
R-free | 0.23090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b5i |
RMSD bond length | 0.008 |
RMSD bond angle | 1.010 |
Data reduction software | XDS |
Data scaling software | SADABS |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.7 (6-FEB-2020)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.980 | 1.920 |
High resolution limit [Å] | 1.830 | 1.830 |
Rmerge | 0.090 | 0.740 |
Number of reflections | 56064 | 7407 |
<I/σ(I)> | 5.7 | |
Completeness [%] | 99.9 | |
Redundancy | 3.39 | |
CC(1/2) | 0.999 | 0.656 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 25% v/v PEG Smear Medium (12.5% w/v PEG 3350, 12.5% w/v PEG 4000, 12.5% w/v PEG 2000, 12.5% w/v PEG 5000 MME) 0.1M SODIUM ACETATE, PH 4.5 |