6IPZ
Fyn SH3 domain R96W mutant, crystallized with 18-crown-6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-05 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.980 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 51.490, 51.490, 51.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.536 - 1.576 |
R-factor | 0.1912 |
Rwork | 0.190 |
R-free | 0.20880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3h0f |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.536 | 1.633 |
High resolution limit [Å] | 1.576 | 1.576 |
Rmerge | 0.063 | 2.542 |
Rmeas | 0.064 | 2.595 |
Rpim | 0.013 | 0.515 |
Number of reflections | 10112 | 988 |
<I/σ(I)> | 29.66 | 0.91 |
Completeness [%] | 99.8 | 98.38 |
Redundancy | 25.6 | 24.9 |
CC(1/2) | 1.000 | 0.565 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295 | 0.08M Sodium acetate trihydrate pH 4.6, 1.6M Ammonium sulfate, 20%(v/v) Glycerol |