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6EXW

Crystal structure of cIAP1-BIR3 in complex with a covalently bound SM

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-4
Synchrotron siteESRF
BeamlineID14-4
Temperature [K]100
Detector technologyCCD
Collection date2013-09-14
DetectorADSC QUANTUM 210
Wavelength(s)0.939
Spacegroup nameP 32 2 1
Unit cell lengths53.799, 53.799, 176.627
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution58.880 - 2.200
R-factor0.1939
Rwork0.191
R-free0.25140
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3mup
RMSD bond length0.013
RMSD bond angle1.651
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0069)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]58.9002.320
High resolution limit [Å]2.2002.200
Rmerge0.0770.551
Rmeas0.1480.630
Number of reflections156552254
<I/σ(I)>7.1
Completeness [%]98.8
Redundancy4.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1EVAPORATION5.929312% PEG 3350, 0.22 M MgCl2, 0.1M BISTris

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