5ZOD
Crystal Structure of hFen1 in apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2016-12-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.950, 61.070, 110.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.431 - 1.900 |
R-factor | 0.198 |
Rwork | 0.197 |
R-free | 0.22620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3q8k |
RMSD bond length | 0.005 |
RMSD bond angle | 0.732 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.431 | 29.431 | 1.950 |
High resolution limit [Å] | 1.900 | 8.500 | 1.900 |
Rmerge | 0.093 | 0.034 | 0.613 |
Rmeas | 0.102 | 0.037 | 0.681 |
Number of reflections | 24041 | 291 | 1645 |
<I/σ(I)> | 13.82 | 35.27 | 2.86 |
Completeness [%] | 99.9 | 96 | 100 |
Redundancy | 5.896 | 5 | 5.3 |
CC(1/2) | 0.998 | 0.998 | 0.873 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 298 | PEG 3350, MgCl2, Tris, KCl |