5ZJF
LDHA-MA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-05-16 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 134.226, 141.495, 144.079 |
Unit cell angles | 90.00, 110.18, 90.00 |
Refinement procedure
Resolution | 37.100 - 2.602 |
R-factor | 0.1839 |
Rwork | 0.181 |
R-free | 0.23870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4okn |
RMSD bond length | 0.008 |
RMSD bond angle | 1.102 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.100 | 2.630 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 153798 | 560845 |
<I/σ(I)> | 19 | |
Completeness [%] | 99.4 | |
Redundancy | 1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 8% Tacsimate (pH 7.0), 20% Polyethylene glycol (PEG) 3350 |