5ZBZ
Crystal structure of the DEAD domain of Human eIF4A with sanguinarine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2017-12-21 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979253 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 73.471, 56.630, 66.324 |
Unit cell angles | 90.00, 116.78, 90.00 |
Refinement procedure
Resolution | 36.492 - 1.309 |
R-factor | 0.194325913427 |
Rwork | 0.194 |
R-free | 0.21042 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zu6 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.251 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.490 | 1.355 |
High resolution limit [Å] | 1.309 | 1.309 |
Rmerge | 0.027 | 0.318 |
Rmeas | 0.038 | 0.450 |
Rpim | 0.027 | 0.318 |
Number of reflections | 53159 | 5697 |
<I/σ(I)> | 12.23 | 2.21 |
Completeness [%] | 90.7 | 97.52 |
Redundancy | 2 | 1.9 |
CC(1/2) | 0.995 | 0.763 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Sodium malonate |