5YYC
Crystal structure of alanine racemase from Bacillus pseudofirmus (OF4)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-19 |
Detector | OXFORD ONYX CCD |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 97.301, 97.314, 112.569 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.766 - 1.801 |
R-factor | 0.1505 |
Rwork | 0.149 |
R-free | 0.17420 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.067 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.058 | 0.586 |
Number of reflections | 99024 | |
<I/σ(I)> | 35.796 | |
Completeness [%] | 99.8 | |
Redundancy | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | 1.4M sodium/potassium phosphate pH 8.2 |