5YL6
Crystal structure of Ofd2 in complex with 2OG from Schizosaccharomyces pombe
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2014-11-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9791 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 71.114, 80.312, 82.607 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.580 - 2.000 |
R-factor | 0.2026 |
Rwork | 0.200 |
R-free | 0.24650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3thp |
RMSD bond length | 0.011 |
RMSD bond angle | 1.091 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 57.580 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.060 |
Number of reflections | 15373 |
<I/σ(I)> | 2.4 |
Completeness [%] | 99.9 |
Redundancy | 8.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 18% MPEG 5000, 0.1M HEPES, pH 7.4 |