5XWU
Crystal structure of PTPdelta Ig1-Ig3 in complex with SALM2 LRR-Ig
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-11 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 90.040, 127.198, 210.919 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.710 - 3.162 |
R-factor | 0.22 |
Rwork | 0.218 |
R-free | 0.25940 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.681 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.180 |
Number of reflections | 41658 |
<I/σ(I)> | 7.48 |
Completeness [%] | 99.8 |
Redundancy | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 7% PEG 20000, 0.1M MES (pH 6.0) |