5X68
Crystal Structure of Human KMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 2012-12-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1 |
Spacegroup name | H 3 |
Unit cell lengths | 176.736, 176.736, 89.434 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 88.370 - 2.100 |
R-factor | 0.211 |
Rwork | 0.209 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.666 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 88.370 | |
High resolution limit [Å] | 2.100 | |
Rmerge | 0.060 | 0.379 |
Number of reflections | 55790 | |
<I/σ(I)> | 25.6 | 2.25 |
Completeness [%] | 96.5 | |
Redundancy | 3.9 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 295 | 0.1 M Tris (pH 8.5), 13% polyethylene glycol 4000, and 15% glycerol |