5WHZ
PGDM1400-10E8v4 CODV Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-09 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.078 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 151.226, 151.226, 200.595 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.552 | 3.740 |
High resolution limit [Å] | 3.549 | 3.550 |
Rmerge | 0.151 | 3.236 |
Rpim | 0.035 | 0.770 |
Number of reflections | 17034 | |
<I/σ(I)> | 14.7 | 1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.3 | 9.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.1 | 277 | 1.68M ammonium sulfate 0.1M sodium cacodylate |