Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL12-2 |
| Synchrotron site | SSRL |
| Beamline | BL12-2 |
| Temperature [K] | 93 |
| Detector technology | CCD |
| Collection date | 2011-06-15 |
| Detector | MARMOSAIC 325 mm CCD |
| Wavelength(s) | 0.97946 |
| Spacegroup name | P 31 |
| Unit cell lengths | 129.703, 129.703, 80.679 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 37.965 - 2.501 |
| R-factor | 0.1871 |
| Rwork | 0.185 |
| R-free | 0.23020 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.003 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 37.965 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 52355 |
| <I/σ(I)> | 19.8 |
| Completeness [%] | 99.1 |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2.4 M ammonium sulfate, 0.1M HEPES pH 7.5 |
