5VSI
CH1/Ckappa Fab mutant 15.1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2015-12-15 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.97931 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 94.279, 60.610, 86.241 |
Unit cell angles | 90.00, 100.59, 90.00 |
Refinement procedure
Resolution | 19.790 - 1.510 |
R-factor | 0.1953 |
Rwork | 0.194 |
R-free | 0.22660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5vr9 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.424 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.900 | 1.590 |
High resolution limit [Å] | 1.510 | 1.510 |
Rmerge | 0.095 | 0.669 |
Number of reflections | 73293 | 10568 |
<I/σ(I)> | 6.4 | 2.2 |
Completeness [%] | 97.7 | 96.9 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294 | see publication |