5VL7
PCSK9 complex with Fab33
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2010-01-13 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97946 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 92.283, 142.523, 253.983 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.750 - 3.500 |
R-factor | 0.201 |
Rwork | 0.199 |
R-free | 0.24500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qtw |
RMSD bond length | 0.008 |
RMSD bond angle | 1.130 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.6) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.630 |
High resolution limit [Å] | 3.500 | 3.500 |
Number of reflections | 21579 | 2114 |
<I/σ(I)> | 11 | 2.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 292 | potassium sodium phosphate |