Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5VEM

Human ectonucleotide pyrophosphatase / phosphodiesterase 5 (ENPP5, NPP5)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCLSI BEAMLINE 08ID-1
Synchrotron siteCLSI
Beamline08ID-1
Temperature [K]100
Detector technologyCCD
Collection date2016-09-17
DetectorRAYONIX MX-300
Wavelength(s)0.9801
Spacegroup nameP 31
Unit cell lengths109.411, 109.411, 134.820
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution44.940 - 2.600
R-factor0.1973
Rwork0.196
R-free0.22660
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.003
RMSD bond angle0.667
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((1.10.1_2155))
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.600
Number of reflections55639
<I/σ(I)>10.5
Completeness [%]100.0
Redundancy5.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.5298MES, PEG 6000, MPD

222624

PDB entries from 2024-07-17

PDB statisticsPDBj update infoContact PDBjnumon