5ULH
Structure of RNF165 in complex with a UbcH5b~Ub conjugate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.278, 60.081, 112.339 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.170 - 1.950 |
R-factor | 0.1903 |
Rwork | 0.189 |
R-free | 0.21740 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 1.790 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 56.170 |
High resolution limit [Å] | 1.950 |
Rmerge | 0.097 |
Number of reflections | 29425 |
<I/σ(I)> | 15 |
Completeness [%] | 99.9 |
Redundancy | 7 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 200 mM potassium thiocyanate, 20% PEG 3350 |