5UE4
proMMP-9desFnII complexed to JNJ0966 INHIBITOR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2010-08-23 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 89.820, 72.945, 77.537 |
| Unit cell angles | 90.00, 106.91, 90.00 |
Refinement procedure
| Resolution | 43.000 - 1.800 |
| R-factor | 0.2003 |
| Rwork | 0.199 |
| R-free | 0.22430 |
| Data scaling software | d*TREK |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 43.000 |
| High resolution limit [Å] | 1.800 |
| Rmerge | 0.052 |
| Number of reflections | 44322 |
| <I/σ(I)> | 10.5 |
| Completeness [%] | 99.7 |
| Redundancy | 3.25 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 5.5 | 293 | 25% PEG 8K 1% glycerol 0.2 M ammonium sulfate 100 mM NaCacodylate |
