5UD7
Crystal Structure of Wild-Type Ig-like Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-24 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 160.664, 160.664, 86.574 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.493 - 2.200 |
R-factor | 0.242745918946 |
Rwork | 0.241 |
R-free | 0.27748 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ud8 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.010 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.15) |
Phasing software | MOLREP |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.493 | 47.490 | 2.260 |
High resolution limit [Å] | 2.200 | 9.590 | 2.200 |
Rmerge | 0.266 | 0.059 | 3.535 |
Number of reflections | 57945 | ||
<I/σ(I)> | 14.1 | ||
Completeness [%] | 100.0 | 99.3 | 100 |
Redundancy | 25.6 | 19.7 | 27.6 |
CC(1/2) | 0.999 | 0.999 | 0.459 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7.9 | 293 | 0.2 M sodium iodide, 1.6 M ammonium sulfate, 0.1 M Tris 7.9 |