5T87
Crystal structure of CDI complex from Cupriavidus taiwanensis LMG 19424
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791519 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 107.097, 107.097, 315.271 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.400 |
R-factor | 0.21613 |
Rwork | 0.215 |
R-free | 0.24697 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.321 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.143 | 0.693 |
Number of reflections | 42464 | |
<I/σ(I)> | 12.84 | 1.45 |
Completeness [%] | 99.7 | 96.3 |
Redundancy | 6.2 | 4.9 |
CC(1/2) | 0.894 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 277 | 0.1 M Mg acetate, 0.1 M Na acetate, 8% PEG 8000 |