5SWZ
Crystal Structure of NP1-B17 TCR-H2Db-NP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 92.231, 100.185, 469.456 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.800 | 2.790 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 2.208 | |
Rmeas | 0.048 | |
Rpim | 0.013 | |
Total number of observations | 272722 | |
<I/σ(I)> | 2 | |
Completeness [%] | 100 | |
Redundancy | 14.8 | |
CC(1/2) | 0.613 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 17% 3350, 0.2 KNaTartrate, 0.1 BTP 7.5 |