5OTT
Extracellular domain of GLP-1 receptor in complex with exendin-4 variant Gly2Hcs/Thr5Hcs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-X |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-24 |
Detector | DECTRIS PILATUS3 R 1M |
Wavelength(s) | 1.54187 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 51.690, 62.920, 118.550 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.382 - 1.920 |
R-factor | 0.1824 |
Rwork | 0.180 |
R-free | 0.20880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zgm |
RMSD bond length | 0.015 |
RMSD bond angle | 1.253 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2689: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.382 | 1.950 |
High resolution limit [Å] | 1.920 | 1.920 |
Rmerge | 0.103 | 1.145 |
Rmeas | 1.193 | |
Rpim | 0.030 | 0.330 |
Number of reflections | 15019 | |
<I/σ(I)> | 19.8 | 2.3 |
Completeness [%] | 99.0 | 97.41 |
Redundancy | 12.9 | 12.66 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Imidazole pH 6.5, 1.0 M Sodium acetate trihydrate |