5OEN
Crystal Structure of STAT2 in complex with IRF9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-02-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.972 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 30.602, 124.037, 51.029 |
Unit cell angles | 90.00, 92.10, 90.00 |
Refinement procedure
Resolution | 32.120 - 2.919 |
R-factor | 0.26 |
Rwork | 0.255 |
R-free | 0.30700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bf5 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.463 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.389 | 2.930 |
High resolution limit [Å] | 2.919 | 2.919 |
Rmerge | 0.194 | 0.898 |
Number of reflections | 7970 | |
<I/σ(I)> | 5.9 | |
Completeness [%] | 96.0 | 98.7 |
Redundancy | 2.8 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 0.2M Potassium formate and 20% PEG3350 |