5O6T
BIRC4 RING in complex with dimeric ubiquitin variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 110 |
Detector technology | PIXEL |
Collection date | 2016-04-28 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.715, 69.972, 109.747 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.970 | 1.577 |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.074 | 0.890 |
Rpim | 0.042 | 0.513 |
Number of reflections | 39227 | 2560 |
<I/σ(I)> | 14.9 | 2 |
Completeness [%] | 100.0 | 96.3 |
Redundancy | 6.4 | 6.5 |
CC(1/2) | 0.663 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.6 | 291 | 0.1 M NaHEPES pH 7.5, 1.4 M tri-Na citrate |