5NSC
Fc DEKK heterodimer variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-07 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.059, 65.442, 78.710 |
Unit cell angles | 90.00, 103.24, 90.00 |
Refinement procedure
Resolution | 76.619 - 2.300 |
R-factor | 0.2273 |
Rwork | 0.225 |
R-free | 0.26470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5dk0 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.725 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.620 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.154 | 0.531 |
Rpim | 0.106 | 0.367 |
Number of reflections | 26379 | 2511 |
<I/σ(I)> | 3.6 | 1.7 |
Completeness [%] | 98.7 | 95.4 |
Redundancy | 2.8 | 2.9 |
CC(1/2) | 0.972 | 0.565 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2 M sodium fluoride, 20% w/v PEG3350 |