5MYV
Crystal structure of SRPK2 in complex with compound 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-02-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97950 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 188.790, 248.990, 146.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.870 - 2.900 |
R-factor | 0.19988 |
Rwork | 0.199 |
R-free | 0.21694 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | pdb id 2X7G |
RMSD bond length | 0.011 |
RMSD bond angle | 1.182 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.870 | |
High resolution limit [Å] | 2.900 | |
Rmerge | 0.138 | 0.957 |
Number of reflections | 75969 | 11061 |
<I/σ(I)> | 9.5 | 1.6 |
Completeness [%] | 99.3 | 99.8 |
Redundancy | 5.8 | 6.1 |
CC(1/2) | 0.993 | 0.840 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.25 | 277.15 | 1.0 M ammonium sulfate and 0.1 M acetate pH 5.25 |