5MF4
Tubulin-Dictyostatin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-12 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.010, 156.510, 179.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.854 - 2.300 |
R-factor | 0.1859 |
Rwork | 0.183 |
R-free | 0.23250 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4i4t |
RMSD bond length | 0.008 |
RMSD bond angle | 0.928 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.854 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.111 | 4.250 |
Number of reflections | 129857 | |
<I/σ(I)> | 18.7 | 0.7 |
Completeness [%] | 99.8 | 98.9 |
Redundancy | 13.4 | 12.6 |
CC(1/2) | 1.000 | 0.262 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.7 | 293 | 5% PEG, 12% GLYCEROL, 30 MM MAGNESIUM CHLORIDE, 30 MM CALCIUM CHLORIDE, 0.1M MES/0.1M IMIDAZOLE |