5ME8
N-terminal domain of the human tumor suppressor ING5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2012-10-04 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.978861 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 135.630, 135.630, 96.670 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.700 | 3.390 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.084 | 0.850 |
Number of reflections | 9086 | |
<I/σ(I)> | 47.54 | 6.2 |
Completeness [%] | 99.9 | 99 |
Redundancy | 7.6 | 35 |
CC(1/2) | 0.972 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 273 | 22 % MPD, 0.1 M MES pH 6.5, 5% PEG 3350 |