5LW9
Crystal structure of human JARID1B in complex with S40563a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.96859 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 142.960, 142.960, 152.470 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 64.915 - 2.300 |
R-factor | 0.1863 |
Rwork | 0.185 |
R-free | 0.21770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a1f |
RMSD bond length | 0.009 |
RMSD bond angle | 1.177 |
Data reduction software | xia2 |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.920 | |
High resolution limit [Å] | 2.300 | 2.360 |
Rmerge | 0.139 | 2.813 |
Number of reflections | 41284 | |
<I/σ(I)> | 15.4 | |
Completeness [%] | 99.8 | 98.4 |
Redundancy | 16.2 | 15.8 |
CC(1/2) | 0.999 | 0.367 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 0.1M HEPES PH 8.0, 0.8M POTASSIUM PHOSPHATE-DIBASIC, 0.8M SODIUM PHOSPHATE MONOBASIC |