5K78
Dbr1 in complex with 16-mer branched RNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-06 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.28081 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.893, 142.673, 215.131 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.336 - 2.640 |
R-factor | 0.1972 |
Rwork | 0.195 |
R-free | 0.24560 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4pef |
RMSD bond length | 0.002 |
RMSD bond angle | 0.545 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 108.000 | 2.780 |
High resolution limit [Å] | 2.640 | 2.640 |
Rmerge | 0.151 | 1.760 |
Number of reflections | 66902 | |
<I/σ(I)> | 10.3 | 1.1 |
Completeness [%] | 99.1 | 99.8 |
Redundancy | 5.6 | 5.8 |
CC(1/2) | 0.988 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | PEG 3350, lithium sulfate, glycerol, bis-tris |