5K0I
mpges1 bound to an inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 31-ID |
| Synchrotron site | APS |
| Beamline | 31-ID |
| Temperature [K] | 78 |
| Detector technology | CCD |
| Collection date | 2014-08-20 |
| Detector | RAYONIX MX-225 |
| Wavelength(s) | .97931 |
| Spacegroup name | H 3 |
| Unit cell lengths | 77.444, 77.444, 123.565 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.650 - 1.300 |
| R-factor | 0.14619 |
| Rwork | 0.145 |
| R-free | 0.15917 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.042 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.650 |
| High resolution limit [Å] | 1.260 |
| Number of reflections | 74628 |
| <I/σ(I)> | 6.9 |
| Completeness [%] | 99.9 |
| Redundancy | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 294 | 0.1 M tris pH 9.4, 36% PEG 1K |
