5JO3
PDE5A for NaV1.7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2010-03-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 55.840, 76.100, 80.920 |
Unit cell angles | 90.00, 102.56, 90.00 |
Refinement procedure
Resolution | 44.000 - 1.490 |
R-factor | 0.18107 |
Rwork | 0.180 |
R-free | 0.20141 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.137 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | BUSTER |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.000 | 1.570 |
High resolution limit [Å] | 1.490 | 1.490 |
Rmerge | 0.115 | |
Number of reflections | 45627 | |
<I/σ(I)> | 12.5 | 5 |
Completeness [%] | 84.8 | 48.8 |
Redundancy | 3.5 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.4 | 293 | 20% PEG 4K 10% Isopropanol 0.1M Hepes pH 7.4 |