5JCP
RhoGAP domain of ARAP3 in complex with RhoA in the transition state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.786, 93.208, 164.283 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.711 - 2.100 |
R-factor | 0.1885 |
Rwork | 0.186 |
R-free | 0.22660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jd0 1a2b |
RMSD bond length | 0.007 |
RMSD bond angle | 0.910 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER (2.5.2) |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 4.520 | 2.100 |
Rmerge | 0.108 | 0.066 | 0.506 |
Number of reflections | 52079 | ||
<I/σ(I)> | 9.5 | ||
Completeness [%] | 99.8 | 99.3 | 99.9 |
Redundancy | 6 | 5.7 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 100 mM MES, 15%(v/v) PEG 550 MME, 4%(v/v) Acetone |