5I4Z

Structure of apo OmoMYC

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-05-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.064
Spacegroup name	P 41 2 2
Unit cell lengths	65.700, 65.700, 149.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.348 - 1.950
R-factor	0.1742
Rwork	0.173
R-free	0.19410
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1nkp
RMSD bond length	0.011
RMSD bond angle	1.135
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.350	2.000
High resolution limit [Å]	1.950	1.950
Rmerge	0.055	0.818
Number of reflections	24551
<I/σ(I)>	17.1	1.7
Completeness [%]	99.3	92.9
Redundancy	5.4	4.4
CC(1/2)	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6	293.15	MES, potassium sodium tartrate