5HRL
The crystal structure of AsfvPolX: 1nt-gap(P) DNA2: dGTP ternary complex.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 124.651, 71.348, 86.922 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.990 - 2.400 |
R-factor | 0.22929 |
Rwork | 0.228 |
R-free | 0.25713 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5hr9 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.403 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 28026 | |
<I/σ(I)> | 28.3 | |
Completeness [%] | 95.2 | |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 277 | 0.1 M BIS-TRIS pH 5.5, 17% w/v PEG 10000, 0.1 M Ammonium acetate |