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5HDH

Crystal structure of human TLR8 with an uncleaved Z-loop

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron sitePhoton Factory
BeamlineAR-NE3A
Temperature [K]100
Detector technologyCCD
Collection date2013-06-01
DetectorADSC QUANTUM 270
Wavelength(s)1.0000
Spacegroup nameH 3 2
Unit cell lengths171.520, 171.520, 301.333
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution45.020 - 2.600
R-factor0.20756
Rwork0.206
R-free0.23944
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.012
RMSD bond angle1.770
Data scaling softwareAimless
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0073)
Data quality characteristics
 Overall
Low resolution limit [Å]45.020
High resolution limit [Å]2.600
Number of reflections49967
<I/σ(I)>17.3
Completeness [%]100.0
Redundancy19.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP293ammonium sulfate, sodium acetate, glycerol

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PDB entries from 2024-11-06

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