5HCC
Ternary complex of human Complement C5 with Ornithodoros moubata OmCI and Dermacentor andersoni RaCI3.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-15 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97935 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.867, 140.284, 211.293 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.570 - 2.590 |
R-factor | 0.2323 |
Rwork | 0.231 |
R-free | 0.26650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cu7 2cm9 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.606 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.600 | 2.680 |
High resolution limit [Å] | 2.590 | 2.590 |
Rmerge | 0.079 | 0.787 |
Number of reflections | 97166 | |
<I/σ(I)> | 9.3 | 1.44 |
Completeness [%] | 99.0 | 100 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 294 | 10% PEG 20K, 2% v/v 1,4 Dioxane, 0.1 M Bicine pH 9.0 |