5GIE
Crystal structure of VDR in complex with DLAM-4P (P21 form)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Collection date | 2012-06-14 |
| Detector | MAR CCD 130 mm |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 65.364, 42.077, 96.802 |
| Unit cell angles | 90.00, 94.55, 90.00 |
Refinement procedure
| Resolution | 38.570 - 2.387 |
| R-factor | 0.2094 |
| Rwork | 0.207 |
| R-free | 0.23420 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.016 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 39.000 |
| High resolution limit [Å] | 2.390 |
| Number of reflections | 19510 |
| <I/σ(I)> | 8.5 |
| Completeness [%] | 100.0 |
| Redundancy | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | Tris-HCl, PEG 8000, NaCl |
