5FZO
Crystal structure of the catalytic domain of human JmjD1C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-30 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 45.320, 110.920, 165.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.460 - 1.840 |
R-factor | 0.1945 |
Rwork | 0.193 |
R-free | 0.23140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ypd |
RMSD bond length | 0.008 |
RMSD bond angle | 1.145 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | DIMPLE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.460 | 1.890 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.130 | 1.500 |
Number of reflections | 72743 | |
<I/σ(I)> | 9 | 1.1 |
Completeness [%] | 99.1 | 97.6 |
Redundancy | 6.6 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 20% PEG3350 -- 10% ETHYLENE GLYCOL -- 0.1M BIS-TRIS-PROPANE PH 8.5 -- 0.2M POTASSIUM CITRATE TRIBASIC |