5FWJ
Crystal structure of human JARID1C in complex with KDM5-C49
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-08 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 |
Unit cell lengths | 60.960, 67.340, 74.730 |
Unit cell angles | 86.71, 76.56, 70.35 |
Refinement procedure
Resolution | 51.232 - 2.100 |
R-factor | 0.1568 |
Rwork | 0.155 |
R-free | 0.18930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a1f |
RMSD bond length | 0.004 |
RMSD bond angle | 0.953 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE: 1.9_1682)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.230 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.080 | 0.270 |
Number of reflections | 95919 | |
<I/σ(I)> | 8.24 | 3.37 |
Completeness [%] | 97.4 | 96 |
Redundancy | 2.8 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 0.1M BIS-TRIS PH 5.5 -- 25% PEG3350 -- 0.25M MAGNESIUM CHLORIDE |