5FMK
Bcl-xL with Bak BH3 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-02-26 |
Detector | ADSC Q210R |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 77.668, 55.459, 61.053 |
Unit cell angles | 90.00, 127.12, 90.00 |
Refinement procedure
Resolution | 19.401 - 1.731 |
R-factor | 0.159 |
Rwork | 0.158 |
R-free | 0.18560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2p1l |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.400 | 1.810 |
High resolution limit [Å] | 1.730 | 1.730 |
Rmerge | 0.040 | 0.300 |
Number of reflections | 21521 | |
<I/σ(I)> | 35.2 | 4.73 |
Completeness [%] | 99.4 | 95.4 |
Redundancy | 3.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.16M CALCIUM ACETATE, 0.08M SODIUM CACODYLATE, PH6.5, 20% GLYCEROL, 14.4% PEG 8000 |