5FCB

Murine SMPDL3A in complex with AMP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-03-21
Detector	RAYONIX MX-300
Wavelength(s)	0.97949
Spacegroup name	C 2 2 21
Unit cell lengths	124.033, 132.381, 79.742
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.574 - 1.550
R-factor	0.1611
Rwork	0.160
R-free	0.18650
RMSD bond length	0.007
RMSD bond angle	0.925
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	41.574
High resolution limit [Å]	1.550
Number of reflections	89133
<I/σ(I)>	19.7
Completeness [%]	93.7
Redundancy	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	citrate, PEG