5FCA

Murine SMPDL3A in presence of excess zinc

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08B1-1
Synchrotron site	CLSI
Beamline	08B1-1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-03-22
Detector	RAYONIX MX300HE
Wavelength(s)	1.28137
Spacegroup name	P 21 21 21
Unit cell lengths	80.137, 123.588, 131.608
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.315 - 1.924
R-factor	0.1757
Rwork	0.175
R-free	0.20420
RMSD bond length	0.011
RMSD bond angle	1.054
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	39.315
High resolution limit [Å]	1.924
Number of reflections	93218
<I/σ(I)>	23.8
Completeness [%]	93.6
Redundancy	25.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	citrate, PEG