5FC6

Murine SMPDL3A in complex with ADP analog AMPCP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-01-21
Detector	RAYONIX MX-300
Wavelength(s)	0.97949
Spacegroup name	C 2 2 21
Unit cell lengths	124.351, 132.888, 80.519
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.399 - 1.658
R-factor	0.1625
Rwork	0.161
R-free	0.19070
RMSD bond length	0.011
RMSD bond angle	1.083
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	45.400
High resolution limit [Å]	1.658
Number of reflections	78590
<I/σ(I)>	15.8
Completeness [%]	99.6
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	citrate, PEG