5DMK

Crystal Structure of IAg7 in complex with RLGL-WE14

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-E
Synchrotron site	APS
Beamline	24-ID-E
Temperature [K]	100
Detector technology	CCD
Collection date	2013-01-13
Detector	ADSC QUANTUM 315
Wavelength(s)	0.979500
Spacegroup name	P 43 21 2
Unit cell lengths	161.765, 161.765, 204.162
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.866 - 2.450
R-factor	0.2138
Rwork	0.211
R-free	0.26000
RMSD bond length	0.009
RMSD bond angle	1.213
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.7.3_928)

Data quality characteristics

	Overall
Low resolution limit [Å]	44.866
High resolution limit [Å]	2.450
Number of reflections	93185
<I/σ(I)>	1.92
Completeness [%]	93.6
Redundancy	2.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	1M Ammonium Citrate