5D7V
Crystal structure of PTK6 kinase domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-03-03 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54789 |
Spacegroup name | P 1 |
Unit cell lengths | 49.718, 76.308, 87.271 |
Unit cell angles | 81.46, 75.92, 74.93 |
Refinement procedure
Resolution | 50.000 - 2.330 |
R-factor | 0.2218 |
Rwork | 0.219 |
R-free | 0.28160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2f4j |
RMSD bond length | 0.008 |
RMSD bond angle | 1.175 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.410 |
High resolution limit [Å] | 2.330 | 2.330 |
Rmerge | 0.113 | 0.443 |
Number of reflections | 50742 | |
<I/σ(I)> | 7.3 | 1.9 |
Completeness [%] | 96.3 | 94.2 |
Redundancy | 2.1 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.23M Diammonium Phosphate, 18% PEG 3350, 1M Lithium chloride |