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5D7O

Crystal structure of Sirt2-ADPR at an improved resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-07-19
DetectorDECTRIS PILATUS 6M
Wavelength(s)1
Spacegroup nameP 21 21 21
Unit cell lengths78.000, 78.170, 114.241
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution49.710 - 1.630
R-factor0.17192
Rwork0.171
R-free0.19070
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3zgv
RMSD bond length0.005
RMSD bond angle1.149
Data reduction softwareMOSFLM
Data scaling softwareAimless
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0071)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]49.7101.660
High resolution limit [Å]1.6301.630
Rmerge0.1140.983
Number of reflections87718
<I/σ(I)>8
Completeness [%]100.0
Redundancy6.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.252770.2 M sodium chloride, 30 % (w/v) PEG 3350, 0.1 M Bis-Tris

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