5D1P
Archaeal ATP-dependent RNA ligase - form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-08 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5414 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.500, 115.304, 91.567 |
Unit cell angles | 90.00, 104.55, 90.00 |
Refinement procedure
Resolution | 29.365 - 2.199 |
R-factor | 0.1937 |
Rwork | 0.192 |
R-free | 0.24130 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 1.306 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 45957 |
<I/σ(I)> | 9.69 |
Completeness [%] | 89.3 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.1 M Tris-HCl (pH 8.5), 0.2 M Lithium Sulfate and 40 % PEG400 |