5CSX
CRYSTAL STRUCTURE OF B-RAF IN COMPLEX WITH BI 882370
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-07-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 49.375, 116.136, 102.423 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.070 - 2.510 |
R-factor | 0.2232 |
Rwork | 0.217 |
R-free | 0.28250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3c4c |
RMSD bond length | 0.009 |
RMSD bond angle | 1.151 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.070 | 2.760 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.082 | 0.441 |
Number of reflections | 10430 | |
<I/σ(I)> | 15.72 | |
Completeness [%] | 99.4 | 99.6 |
Redundancy | 5.2 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG 3350 |